1) solid-state method
固相法
1.
Preparation of PTh/TiO_2 nanocomposite by solid-state method and its photocatalytic activity under visible light irradiation
固相法制备PTh/TiO_2复合纳米粉可见光催化剂
2.
Neodymium-doped gadolinium gallium garnet (Nd:GGG) precursor and ceramic were prepared by the liquid phase co-precipitation or solid-state methods,and properties of samples prepared by these methods were studied.
比较了用液相沉淀法或固相法合成的粉体以及最终制得的掺钕钆镓石榴石(neodymium-doped gadolinium gallium garnet,Nd:GGG)陶瓷的性能。
3.
The layered LiNi1/3Mn1/3Co1/3O2 cathode material for Li-ion batteries was synthesized by high temperature solid-state method.
采用高温固相法合成出层状锂离子电池正极材料LiNi1/3Mn1/3Co1/3O2。
2) solid state reaction
固相法
1.
Synthesis of negative thermal expansion material ZrW_2O_8 powders using solid state reaction;
固相法合成负热膨胀性粉体ZrW_2O_8
2.
25O2compounds were syn-thesized by a solid state reaction using LiOH.
H2O和Ni,Co,Mn过渡金属或其氧化物为原料,采用固相法制备了锂离子电池正极材料LiNi0。
3.
Yttria precursor powder is synthesized by solid state reaction of YCl3·6H2O with Na2C2O4.
6H2O和Na2C2O4为反应物,固相法制备氧化钇纳米粉体前驱体,用差热-热重法分析前驱体的分解过程,用X射线衍射和透射电镜对产物的组成、粒度和形貌进行表征。
3) Solid Phase Method
固相法
1.
Polypropylene Modified by Org-Clay Prepared through Solid Phase Method;
固相法制备有机黏土改性聚丙烯
2.
Tin phthalocyanine and its sulfonated derivated were synthesized by solid phase method.
以苯酐和氯化亚锡为原料,采用固相法合成锡酞菁(SnPc),再和发烟硫酸反应合成磺化锡酞菁(SnPcS)。
3.
These methods include solid phase method(mechanical pulverization method,solid phase reaction method),liquid phase method(precipitation method,hydrothermal reaction method,micro-lacteous method,sol-gel method,hydrolysis method,solvent vaporization method,electrochemistry method) and gas phase method(atmosphere vaporization method,gas phase c.
综述了纳米材料的主要制备方法,包括固相法(机械粉碎法、固相反应法)、液相法(沉淀法、水热法、微乳液法、溶胶凝胶法、水解法、溶剂蒸发法、电化学法)和气相法(气体中蒸发法、气相化学反应法、溅射法、流动油面上真空沉积法、金属蒸气合成法)等。
4) solid-state reaction
固相法
1.
Compared with liquid phase reaction,the advantages of solid-state reaction.
采用低温固相法与常规液相法合成系列磷酸铵复盐NH4MPO4。
2.
Co_3O_4 nanoparticles were synthesized from Co(NO_3)_2·6H_2O and NaOH by solid-state reaction.
6H2O和NaOH为原料,用固相法合成了Co3O4纳米微粒。
3.
Orthorhombic LiMnO2 material was synthesized via a one-step solid-state reaction and characterized, and the conversion process of mixture at calcination condition and the mechanism of intercalation reaction were confirmed.
用一步固相法合成了斜方锰酸锂,对其进行了表征并确定了前驱体化合物烧结中的转变过程,以及相互化合间的烧结机制。
5) solid state method
固相法
1.
Application of clay modified with solid state method in polypropylene;
固相法插层改性黏土在PP中的应用
2.
Cathode material LiMn_(1/3)Ni_(1/3)Co_(1/3)O_2 for lithium ion battery prepared by solid state method;
固相法制备锂离子电池正极材料LiMn_(1/3)Ni_(1/3)Co_(1/3)O_2
3.
Pilot test production on doped and compounded LiMn_2O_4 by solid state method
固相法中试合成掺杂复合的LiMn_2O_4
6) solid state reaction method
固相法
1.
In this paper, zirconium tungstate was synthesized using solid state reaction method with zirconium dioxide and tungstate trioxide as raw materials.
本文采用ZrO2和WO3为原料,以固相法制备ZrW_2O_8,以X射线粉末衍射仪对试样进行物相分析。
2.
Blue-emitting long-lasting phosphors Sr2Al6O11∶Eu2+,Dy3+ were synthesized by conventional solid state reaction method.
采用传统的高温固相法合成了蓝色长余辉发光材料Sr2Al6O11∶Eu2+,Dy3+,系统研究了烧结温度对Eu2+和Dy3+共掺杂蓝色铝酸锶长余辉材料物相及发光性能的影响。
3.
The earth phosphors SrBPO5:Eu were prepared by combustion synthesis, other than the solid state reaction method, the pure borophosphate phase were gotten in 900 ℃ by combustion synthesis that was 100 ℃ lower than the solid state reaction method.
结果表明,用固相法需在1000℃才能得到纯的物相,燃烧法900℃即可制得,并且节省了反应时间,产物发光亮度也很高。
补充资料：固相萃取法
分子式：
CAS号：
性质：根据被萃取组分与样品基质及其他成分在固定相填料上作用力强弱的不同，使之彼此分离的技术。首先用适当的溶剂将固相萃取吸附剂润湿，然后加入一定体积的被处理样品溶液，使其完全通过吸附剂，让溶液中被测组分保留在吸附剂上，而大量的溶剂和其他不易保留在固相萃取吸附剂上的组分完全流出，再加入适当的洗涤剂从固相萃取吸附剂上除去其他不需要的组分，最后用洗脱液把保留在固相萃取吸附剂上需要测定的组分洗脱下来，直接供测定使用。具有快速、高效、重复性好、选择性好等优点。固相萃取装置主要有柱型和盘状薄膜型，通常是一次性使用，此技术在环境样品前处理的应用主要是对水样的处理，也可用于大气样品的前处理。此法与色谱分析的在线联用越来越广泛，如柱型固相萃取-高效液相色谱的在线联用、固相萃取-气相色谱的在线检测联用等。
CAS号：
性质：根据被萃取组分与样品基质及其他成分在固定相填料上作用力强弱的不同，使之彼此分离的技术。首先用适当的溶剂将固相萃取吸附剂润湿，然后加入一定体积的被处理样品溶液，使其完全通过吸附剂，让溶液中被测组分保留在吸附剂上，而大量的溶剂和其他不易保留在固相萃取吸附剂上的组分完全流出，再加入适当的洗涤剂从固相萃取吸附剂上除去其他不需要的组分，最后用洗脱液把保留在固相萃取吸附剂上需要测定的组分洗脱下来，直接供测定使用。具有快速、高效、重复性好、选择性好等优点。固相萃取装置主要有柱型和盘状薄膜型，通常是一次性使用，此技术在环境样品前处理的应用主要是对水样的处理，也可用于大气样品的前处理。此法与色谱分析的在线联用越来越广泛，如柱型固相萃取-高效液相色谱的在线联用、固相萃取-气相色谱的在线检测联用等。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条