1) econazole
氯氧甲苯咪唑
1.
To investigate apoptosis of mouse leukemia cell (WEHI-3) induced by econazole and its mechanism, apoptosis induced by econazole was examined by flow cytometry, while free calcium ([Ca 2+]i) was determined by Fura-2 fluorescein load techinique.
为了研究氯氧甲苯咪唑(econazole)诱导鼠粒单核白血病细胞WEHI3凋亡的机制,利用AnnexinⅤ/PI双染实验测定细胞凋亡,Fura2荧光负荷技术检测细胞内游离钙离子浓度([Ca2+]i),并抽取WEHI3细胞内质网部分蛋白,利用Westernblot测定caspase7、caspase12的蛋白表达。
2) zirconium oxychloride
氯氧化锆
1.
ZnO green phosphor preparation process by the thermal oxidation of zinc sulfide with zirconium oxychloride as additive is investigated.
研究以氯氧化锆为添加剂的硫化锌热氧化法合成ZnO绿色荧光粉的过程。
2.
The acid property of zirconium oxychloride was characterized by means of DTA and FT-IR spectra of pyridine absorbed on the surface.
采用DTA和吸附吡啶的FT-IR表征氯氧化锆的表面酸性,用Hamm ett指示剂测定其酸强度,以催化合成环己酮2,3-丁二醇缩酮为探针反应优化缩酮反应条件,并考察它对其他缩酮反应的催化活性,比较了不同催化剂对缩酮活性的影响。
3.
This paper introduced the traditional washing technology of zirconium oxychloride, researched and tested the washing and eliminating technologies of silica under most kinds of conditions, and educed the best technology for washing and eliminating of silica.
本文研究了传统的氯氧化锆水洗工艺,提出了水料倒置的水洗除硅路线。
3) chlorine oxidation
氯氧化
1.
The treatment of pharmaceutical wastewater containing antibiotic was performed by both photocatalysis oxidation and chlorine oxidation.
采用光催化氧化法和氯氧化法对抗生素制药废水进行了研究,探讨了上述过程中光照时间、通气条件、初始pH值及投加有效氯量等因素对抗生素制药废水处理效果的影响。
2.
A new technique to deal with methyl mercaptan by chlorine oxidation was introduced.
介绍了用氯氧化法处理化工生产单元中排放出的甲硫醇尾气新技术。
3.
Neutralization chlorine oxidation electrochemical reaction catalytic oxidation process has been used in the treatment of the mixed wastewater from basic and weak acid dyestuff production,achieving reduction of COD from 14460 mg/L to 215 mg/L and that of colority from 50000 times to less than 10 times.
采用“中和 -氯氧化 -电化学反应 -催化氧化”组合工艺处理碱性、弱酸性染料混合废水 ,可使混合废水的 COD由 1 4560 mg/L降至 2 1 5mg/L,色度由 50 0 0 0倍降至 1 0倍以下。
4) phosphorus oxychloride
三氯氧磷
1.
A new technology of continuous preparing phosphorus oxychloride and thionyl chloride;
连续联合制备氯化亚砜和三氯氧磷新工艺
2.
Review on the production and application of phosphorus oxychloride and its derivatives;
三氯氧磷及其衍生产品的生产及应用综述
3.
Research on clear technique to synthesize phosphorus oxychloride;
三氯氧磷清洁生产工艺的研究
5) phosphoryl chloride
三氯氧磷
1.
Economic evaluation of simultaneous production of sulfinyl chloride and phosphoryl chloride;
氯化亚砜联产三氯氧磷工艺的经济评价
2.
Application of ESI-MS in the Reaction of Amino Acids and THF with Phosphoryl Chloride;
ESI-MS应用于三氯氧磷与氨基酸及四氢呋喃反应的研究
3.
Using phosphoryl chloride as catalyst, 5,6-O-isopropylidene ascorbic acid was prepared by the reaction of Vc and acetone, then the product was treated with phosphoryl chloride to produce Magnesium L-ascorbate-2-phosphate.
在三氯氧磷催化剂作用下,Vc首先与丙酮反应生成5,6-O-异丙叉-L-抗坏血酸(IAA),再与三氯氧磷发生磷酰化反应合成得到。
6) phosphorous oxychloride
三氯氧磷
1.
Two novel bi-dodecyl bi-phosphate compounds, DGDP and PDP were synthesized from phosphorous oxychloride, diethylene glycol (hydroquinone) and dodecanol via the esterification of two steps and the hydrolization of one step, and were purified by recrystallization in absolute ethyl alcohol.
利用三氯氧磷与一缩二乙二醇或对苯二酚反应之后,再与正十二醇反应,最后通过水解,合成了2种新型双十二烷基双磷酸酯(DGDP,PDP)。
2.
Pentaerythritol diphosphonate of melamine (PDM), a novel intumescent flame retardant, was synthesized from water, melamine and pentaerythritol diphosphonate dichloride (PDD) which was prepared from pentaerythritol and phosphorous oxychloride in the absence of organic solvent.
采用非溶剂法经过二步反应合成了膨胀型阻燃剂季戊四醇二磷酸酯蜜胺盐 ( PDM) ,首先三氯氧磷和季戊四醇反应得到季戊四醇二磷酸酯二磷酰氯 ( PDD) ,然后 PDD再与水、蜜胺反应 ,制备得到 PDM。
参考词条
补充资料:1-氯-4-甲苯
分子式:C7H7Cl
分子量:126.59
CAS号:106-43-4
性质:无色油状液体。熔点7.6℃,沸点162℃,44℃(1.33kPa),相对密度1.0697(20/4℃),折射率1.5150,燃点>500℃,闪点49℃。微溶于水。可溶于乙醇、乙醚、丙酮、苯及氯仿。可进行水蒸气蒸馏。其甲基可以氧化而得相应的醛和酸。有特殊气味。
制备方法:1.由对甲苯胺经重氮化、置换而得。将对甲苯胺和盐酸加入反应锅中搅拌加热,至60℃溶解后,冷却至15℃以下,滴加亚硝酸钠溶液。到达终点后继续搅拌0.5h。加入氯化亚铜盐酸溶液,在室温搅拌3h。然后升温至60℃保持0.5h,冷至室温静置分层,弃去酸水层,用水洗至中性,过滤,得对氯甲苯。反应所用的氯化亚铜可按下法制备:将硫酸铜和氯化钠加入水中,搅拌加热至40℃溶解,加入液碱和焦亚硫酸钠溶液,析出沉淀物,静置分层,分去上层废液,沉淀用水浸洗,加盐酸溶解,即得氯化亚铜盐酸溶液。原料消耗定额:对甲苯胺(95%)897kg/t、亚硝酸钠533kg/t、盐酸2435kg/t。2.由甲苯进行芳环氯化制得。
用途:有机合成原料。合成医药、农药和染料的中间体,如合成乙胺嘧啶,芬那露的中间体,也用作溶剂。
分子量:126.59
CAS号:106-43-4
性质:无色油状液体。熔点7.6℃,沸点162℃,44℃(1.33kPa),相对密度1.0697(20/4℃),折射率1.5150,燃点>500℃,闪点49℃。微溶于水。可溶于乙醇、乙醚、丙酮、苯及氯仿。可进行水蒸气蒸馏。其甲基可以氧化而得相应的醛和酸。有特殊气味。
制备方法:1.由对甲苯胺经重氮化、置换而得。将对甲苯胺和盐酸加入反应锅中搅拌加热,至60℃溶解后,冷却至15℃以下,滴加亚硝酸钠溶液。到达终点后继续搅拌0.5h。加入氯化亚铜盐酸溶液,在室温搅拌3h。然后升温至60℃保持0.5h,冷至室温静置分层,弃去酸水层,用水洗至中性,过滤,得对氯甲苯。反应所用的氯化亚铜可按下法制备:将硫酸铜和氯化钠加入水中,搅拌加热至40℃溶解,加入液碱和焦亚硫酸钠溶液,析出沉淀物,静置分层,分去上层废液,沉淀用水浸洗,加盐酸溶解,即得氯化亚铜盐酸溶液。原料消耗定额:对甲苯胺(95%)897kg/t、亚硝酸钠533kg/t、盐酸2435kg/t。2.由甲苯进行芳环氯化制得。
用途:有机合成原料。合成医药、农药和染料的中间体,如合成乙胺嘧啶,芬那露的中间体,也用作溶剂。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。