2) Solvothermal-thermal decomposition method
溶剂热-热分解法
3) hydrolysis solvothermal method
水解溶剂热法
1.
Nanometer titanias in different crystal structures with high specific surface area have been prepared by the hydrolysis solvothermal method usi.
本文以钛酸丁酯为原料，在酸性条件下，通过醇盐水解溶剂热法可控地合成了具有较高比表面积的金红石型和锐钛矿型混合晶型的纳米TiO_2粉体。
5) solvothermal
溶剂热法
1.
Emulsifier-free poly(methyl methacrylate-styrene)[P(MMA-St)] cationic nanoparticles with an average diameter of about 40 nm were prepared in an acetone-water medium using 2,2-azobis(2-methylpropionamidine) dihydrochloride(AIBA) as the initiator by solvothermal method.
运用溶剂热法,以丙酮-水为分散介质,偶氮二异丁基脒盐酸盐(AIBA)引发苯乙烯(St)和甲基丙烯酸甲酯(MMA)共聚,制得粒径约为40nm的无皂阳离子聚(苯乙烯-甲基丙烯酸甲酯)纳米胶乳粒子[P(MMA-St)],其结构经TEM,FT-IR,TG和DTA表征。
2.
7O3 nanoparticles have been successfully synthesized by hydrothermal and solvothermal methods, and the synthesis mechanism was discussed.
采用传统的水热法和混合溶剂热法制备了高纯的四方相KTN纳米粉体KTa0。
3.
In the first part of this paper, several nano-sulfides with special structure andmorphology had been synthesized successfully by solvothermal method using thequaternary ammonium salt of 2-undecyl-1-dithioureido-ethyl-imidazoline (SUDEI) asthe surfactant, and characterized by TEM、SEM、XRD、EDS and IR, respectively.
本论文的第一部分是以月桂酸硫脲咪唑啉季铵盐(SUDEI)为表面活性剂，溶剂热法制备了几种具有特殊形貌与结构的纳米硫化物，分别用TEM、SEM、XRD、EDS、IR对产物进行了表征，探讨了该表面活性剂对在介观尺度下的有机-无机杂化凝聚体形成的作用。
6) Solvothermal synthesis
溶剂热法
1.
This paper focuses on the novel properties of magnetics, field emission, electrochemistry, photoelectrochemistry and catalysis of well-ordered nanowire/rod/tube array materials, which are synthesized by vapor-liquid-solid method, vapor-solid method, templates and Solvothermal synthesis method.
概述了有序纳米线/棒/管阵列的性质、应用及制备方法的研究进展,着重介绍了有序纳米线/棒/管阵列材料的制备方法如气相-液相-固相生长法、气相-固相生长法、模板法和溶剂热法,以及阵列材料在磁、场发射、激光、电化学、光电化学和催化方面所具有的独特性质与应用,展望了该领域的研究前景。
2.
There are a variety of methods for the preparation of PZT, such as coprecipitation, solvothermal synthesis and sol-gel process, but the prepared PZT products are mostly in the size of micrometer-scale.
本文在前人工作的基础上，利用sol-gel法和溶剂热法的优点：可以使用的所有高纯原料均可处于溶液状态，在分子或原子水平上实现充分均匀混合，探讨了在非水溶剂中sol-gel法和溶剂热法在PZT粉体制备中的应用，并分别探讨了PZT制备的规律及特点： 1。
补充资料：碘化物热分解法
利用化学迁移反应原理，由粗金属通过碘化物热分解制取高纯金属的一种精炼方法。1925年首先由德国人范阿克耳(A.E.Van Arkel)和德布尔(J.H.de Boer)应用于钛和锆的提纯,因此也称为范阿克耳（Van Arkel）法。由于碘在过程中循环使用而不消耗，也有人称之为"催化蒸馏"（catalytic distillation）法。目前此法已成功地应用于小量高纯金属如钛、锆、铪、钒、硅、铬、铀、钍等的制取，但工业规模生产时成本较高。
参考书目
W.D.Jamrack, Rare Metals Extraction by ChemicalEngineering Techiques,Pergamon,London,1963.
参考书目
W.D.Jamrack, Rare Metals Extraction by ChemicalEngineering Techiques,Pergamon,London,1963.
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条